QBA-QBD-QBH Operating Manual Ver 12 Oct 2012

Contents

1. 2. 3. 4.

Safety Operation of QBA Operation of QBD and QBH ranges User features QBD and QBH ranges Timer Alarm Offset Probe selection Delay start / stop Calibration Programming (QBH only)

5. Maintenance 6. Guarantee and service 7. Accessories 8. Specification 9. Compliance 10. Declaration of Conformity

2 3 4 6 6 7 7 8 9 10 11 12 13 14 15 16 Inside rear cover

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QBD, QBA, QBH, Operating Manual www.grantinstruments.com

1. Safety The following symbols mean:Caution: Read these operating instructions fully before use and pay particular attention to sections containing this symbol. Caution: Surfaces can become hot during use. Always observe the following safety precautions Do not check the temperature by touch. Use a thermometer. Do not touch surfaces which become hot during high temperature operation. Use only as specified by the operating instructions, or the intrinsic protection may be impaired. To reduce the risk of eye injury during high temperature operation, use safety goggles or spectacles. After transport or storage in humid conditions, dry out the unit before connecting it to the supply voltage. During drying out the intrinsic protection may be impaired. Connect only to a power supply with a voltage corresponding to that on the serial number label at the rear of the unit. Ensure that the mains switch and power plug are easily accessible during use. Connect only to a power supply which provides a safety earth (ground) terminal. Before moving, allow to cool and disconnect at the power supply socket. If liquid is spilt inside the unit, disconnect it from the power supply and have it checked by a competent person. It is the user’s responsibility to carry out appropriate decontamination if hazardous material is spilt on or inside the equipment. Clean the unit only with a damp cloth. Do not use chemical cleaning agents. Before using any cleaning or decontamination method except those recommended in this manual, users should check with Grant Instruments that the proposed method will not damage the equipment. The unit must be placed on a level, non-flammable surface away from flammable materials and ensuring that all ventilation slots in the base are clear from obstructions. Disconnect the mains before removing the outer cover. Note there are no user serviceable parts inside in the unit. Use appropriate vessels / tubes for temperature required. The unit is for indoor use only. Check that the environmental conditions of the laboratory are within the limits given in Section 5. Do not use in fume cupboards containing corrosive atmospheres. QBD, QBA, QBH, Operating Manual

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EN

2. Operation of QBA

Mains inlet

Extractor tool storage bracket Removable block

Heater indicator Power indicator

Mains switch Control knob

1. 2.

Unpack the unit carefully and retain packaging for future shipment or storage. The pack includes: Block heater, Mains cable, Operating instructions, Extractor tool. 3. Plug the mains cable into the socket at the rear of the unit and position to allow easy access to the power switch and connector. 4. Fit the desired block(s) into the heater well. Ensure that the heater bed and the bottom of the blocks are clean in order to ensure good thermal contact between heater and blocks resulting in optimal temperature control performance. 5. Turn the unit on by pressing the mains switch on the front of the unit. The power light will illuminate. 6. Turn the control knob to the desired temperature. 7. The block heater will now begin to heat the blocks. The heater light will illuminate continuously during the heating phase but will begin to flash when the set temperature is approached. 8. Allow the block(s) to stabilise at the set temperature before use. 9. If a more accurate temperature setting is required, use a calibrated thermometer. Place in the thermometer hole in the block and adjust the set temperature accordingly. N.B. Allow time for block to stabilise between each adjustment. 10. To turn the unit off press the mains switch on the front. Allow the unit to cool before completing any maintenance. Extractor tool: The extractor tool enables the user to remove blocks safely and easily. The tool can be stored on the rear of the unit in the mounting bracket provided. The tool should be screwed tightly into the threaded hole/holes in the block and then the block lifted out. N.B. One tool is provided with the unit for use with single blocks. A second tool is provided with the double size blocks which require the use of two tools.

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3. Operation of QBD,QBH

Display

Mains inlet

Extractor tool storage bracket

Removable block Heater indicator Fault indicator Control knob

Mains switch

(F)unction & (S)elect buttons

1. 2. 3. 4. 5. 6. 7. 8. 9.

Unpack the unit carefully and retain packaging for future shipment or storage. The pack includes: Block heater, Mains cable, Operating instructions, Extractor tool. Plug the mains cable into the socket at the rear of the unit and position to allow easy access to the power switch and connector. Fit the desired block(s) into the heater well. Ensure that the heater bed and the bottom of the blocks are clean in order to ensure good thermal contact between heater and blocks resulting in optimal temperature control performance. Turn the unit on by pressing the mains switch on the front of the unit. The display will illuminate showing the current temperature of the block. Press the ‘S’ button and adjust the set temperature using the knob. Press ‘S’ to select the temperature or press ‘F’ to exit without changing the value. The block heater will now begin to heat the blocks. The heater light will illuminate continuously during the heating phase but will begin to flash when the set temperature is approached. Allow the block(s) to stabilise at the set temperature before use. To turn unit off, press the mains switch on the front. The set temperature will be stored in memory. Allow unit to cool before completing any maintenance.

Extractor tool: The extractor tool enables the user to remove blocks safely and easily. The tool can be stored on the rear of the unit in the mounting bracket provided. The tool should be screwed tightly into the threaded hole/holes in the block and then the block lifted out. N.B. One tool is provided with the unit for use with single blocks. A second tool is provided with the double size blocks which require the use of two tools.

QBD, QBA, QBH, Operating Manual

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EN

Heating Error Detection (QBDQBH) If the processor detects an error in heating the fault light will illuminate, the buzzer will beep and the display will flash . To reset this fault; switch the unit off and on. If the fault re-occurs contact your local service agent or Grant Instruments: contact details can be found towards the rear of this manual.

Adjustable Over-Temperature Protection Device (QBH) The QBH is fitted with an adjustable over-temperature protection device at the rear of the unit. This device is designed to protect the sample not the user from harm. If operated it will display the same fault as above. To set the device use the following procedure: a) Turn the knob of the protection thermostat to maximum (clockwise) b) Set the control temperature to 2°C above the desired operating temperature and wait for the temperature to stabilise c) Slowly turn the knob down until a click is heard and -ot- is displayed d) Reset the control temperature to the desired operating temperature

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4. User features - QBD, QBH

The digital range of products also contain the following user features: Timer Alarm Offset Probe selection Delay Start and Stop Calibration Programming (QBH only)

Timer The timer is used to count down a time period in the range of 1 to 999 minutes. A buzzer signifies time up, but the heater control is not affected. 1 2 3 4 5 6 7 8 9

Press F to enter main menu. Rotate control knob until display shows . Press S to select timer control. Display will show  or . Rotate knob to desired state and press S to select state. If  is selected the display will flash and show number of minutes. Rotate the control knob until the desired value is displayed and press S to select. If  is selected the display will return to the actual temperature. If the timer is set the display will alternate between actual temperature and time left on the timer. Once the timer has counted down to zero the buzzer will sound and the display will alternate between  and actual temperature1. To cancel the buzzer press either F or S key. The buzzer will cancel automatically after 5 minutes. If the main power to the unit fails the timer will revert to 2.

Notes: 1 The heater control is not affected by the timer, normal operation continues. 2 The timer value will be retained in memory after the main power has been turned off.

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EN

Alarm The alarm is a deviation alarm, settable from 0.5 to 10 ºC. If the actual temperature deviates from the set point by more than the value selected the alarm will sound and the fault lamp illuminates. It is only activated once the actual value has been within ± 0.2 ºC of the set value for 2 minutes. It does not affect the normal operation of the unit. 1 2 3 4 5 6 7 8 9 10

Press F to enter main menu. Rotate control knob until display shows . Press S to select alarm control. Display will show  or . Rotate knob to desired state and press S to select. If  is selected the display will flash and show the current set value. Rotate control knob until desired value is shown. (The alarm limit is ± 0.5 oC to ±10.0oC) If  is selected the display will return to the actual temperature. Press S to set alarm state once the desired value has been selected. The display will return to actual temperature. No indication is given that the alarm is set. If the temperature is outside the limit set for more than 10 seconds, the buzzer will sound and the display will alternate between actual temperature and . To reset the alarm press either F or S key. If the alarm conditions still exist the alarm will re-activate after 10 seconds. To disable the alarm feature select  at point 4 above.

Note: The alarm value and set state condition are retained in memory.

Offset The offset feature allows the user to change the temperature from +3ºC to –7 ºC in order to allow single point calibration. 1 2 3 4 5 6

Press F to enter main menu. Rotate control knob until display shows . Press S to select offset control. The display will flash and show current value. Rotate the control knob until desired value is shown. Press S to confirm the offset value. To cancel the offset, set the value to ..

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Probe Selection By using the optional external probe, it is possible to control the temperature of a sample, a dummy sample or the block directly. Ensure the probe is maintained in contact with either a sample or the block during the course of the experiment. Failure to maintain this contact could result in the probe monitoring an air temperature or, another non-specific temperature. This could result in the temperature exceeding the set point and an error condition occurring (see “Errors” below). Grant has provided this function to protect accidental operation when the external probe has been ‘selected’ but is not used. When selected the external probe may be calibrated by the procedure described on page 10. To select the external probe, complete the following procedure: 1 2 3 4 5 6

Press F to enter main menu. Rotate control knob until display shows . Press S to select probe selection. The display will show which probe type is currently selected.  for internal and  for external. Rotate the control knob until the desired probe is shown. Press S to select the desired probe.

Errors: 1.

2.

The external probe should be plugged in before it is selected. If the probe is not connected to the unit or disconnected the message  will be displayed. If a difference of 40°C or more is detected between the internal and external probe then  will be displayed. - This condition might occur if the external probe is not in direct contact with a sample, a dummy sample or the block. - This error can also occur if the external probe is placed in a cool sample which is then placed in a pre-warmed block. To remove an error 3, ensure the external probe is indeed in direct contact with the chosen target and there is not a difference of more than 40 oC between the block (measured by the internal probe) and the external probe. As the sample heats-up, the heater will switch on again as the difference becomes less than 40oC. Therefore the user can wait and err3 will clear. N.B. Should experimental conditions require a difference of 40oC or more between the block and the external probe, please contact Grant to discuss other options.

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Delay Start and Stop The delay start and stop provides a means of turning the heater control on or off after a specified period of time. 1 2 3 4 5 6 7

Press F to enter main menu. Rotate control knob until display shows . Press S to select delay control. Display will show  or , rotate knob to desired state. Press S to select state. If  is selected the display will show either (delayed start) or  (delayed stop). Using the control knob select which type of delay is required. Press S to select. The display will flash and show the number of minutes delay. Rotate the control knob until the desired value is displayed and press S to select.

Notes: 1 2

During delayed start the display will alternate between  and the actual temperature. During delayed stop the unit will continue to respond as normal. Once the delayed period has expired the temperature control will be turned off and the display will alternate between  and the actual temperature. To return to normal operation press either the S or F keys.

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Calibration The calibration procedure allows the user to calibrate the unit over a wide temperature range. Note that the probe used will be the probe selected as described on page 8. A calibrated thermometer will be required to measure the temperature of the block. The adjusted readings entered must be within ± 5ºC of the original reading. 1 2 3 4 5 6 7 8 9 10 11 12 13

14 15 16 17 18 19

Set the temperature of the unit to 35°C in the normal manner and allow the unit to stabilise. Press F to enter main menu. Rotate control knob until display shows . Press S to select. The display will show  for one second then . Rotate to a value of 0004 and press S to select. Rotate the control knob until the display shows . Press S to select. The display will show the current temperature value. Using the control knob change the value to match that of the calibrated thermometer. Press S to select the new value. The display will revert to the non-adjusted actual temperature. Set the temperature of the unit to 75°C and allow the unit to stabilise. Press F to enter main menu. Rotate control knob until display shows . Press S to select. The display will show  for one second then . Rotate to a value of 0004 and press S to select. Rotate the control knob until the display shows . Press S to select. The display will show the current temperature value. Using the control knob change the value to match that of the calibrated thermometer. N.B. If the reading is over 3 degrees out the unit will continue to flash the display. In this case turn the unit off and allow to cool. Then remove the blocks and clean the heater bed and bottom of the blocks and start the procedure again. Press S to select the new value. The display will revert to the non-adjusted actual temperature. Press F to enter main menu. Rotate control knob until display shows . Press S to select . The display will show  for one second then . Rotate to a value of 0004 and press S to select. Rotate the control knob until the display shows . Press S to select. The display will now display the actual adjusted temperature using the calibration values entered.

To return to factory settings complete the following: 1 Press F to enter main menu. 2 Rotate control knob until display shows . Press S to select. 3 The display will show  for one second then . Rotate to a value of 0004 and press S to select. 4 Rotate the control knob until the display shows . Press S to select.

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EN

Programming (QBH with external probe only) The QBH is capable of running a simple program consisting of three temperature and time segments and an end phase. All the temperature/time segments must be set even if only 2 steps are required. An external probe must be fitted to edit or run a program. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15

16 17 18 19 20

Press F to enter main menu. Rotate control knob until display shows . Press S to select. Rotate the control knob to show  or . Press S to select state. (On or Off will return the display to actual temperature. On runs the program, Off returns to normal operation). If is selected the display will show (section 1) then  (set point). Press S to select. The display will flash and show the current set value. Rotate the control knob until the desired value is displayed and press S to select. The display will show t (time). Press S to select. The display will flash and show the time in minutes. Rotate the control knob until the desired value is displayed and press S to select. The display will show  (section 2). Repeat steps 6 to 10 above for sections 2 and 3. The display will show  (section 4), press S to select. The display will show  (buzzer) press S to select. By rotating the control knob the display will show or. Press S to select state of buzzer when the program finishes (it will sound for 1 minute). The display will show (heater control). Press S to select. By rotating the control knob the display will show or. Press S to select state of heater control when the program finishes. If Off is selected the heater is switched off after the last step and there is no temperature control. If On is selected the unit will return to normal operation. The unit is now programmed; to run the program: Press F to enter main menu. Rotate control knob until display shows . Press S to select. By rotating the control knob the display will show  or . Select On and press S. (If external probe is not selected  will be displayed). To cancel the program complete steps 18 to 21 but select Off.

Notes: 1.

2.

When running a program the display will alternate as follows: When heating up the display will alternate between  and the actual temperature. When temperature has been achieved the display will alternate between time left, step number and actual temperature. The time count down for each step is only started once the actual temperature is within 1 ºC of the set temperature.

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5.Maintenance All products covered in this manual are designed to comply with IEC61010-1 and can be flash tested. Some are fitted with radio frequency interference suppressers. Therefore it is recommended that only a D.C. test be performed. No other routine service is required.

Cleaning The case can be cleaned with a damp cloth after disconnection. Do not use solvents. Before using any decontamination or cleaning method except that recommended, check with our Service Department that the proposed method will not damage the equipment.

Replacement of fuses Disconnect from the power supply socket. Remove the IEC power plug from the rear of the unit. Pull out the fuse drawer, replace the fuse with the correct type, and replace the fuse holder. The fuses are ceramic quick acting, rated: Model

Fuse Rating (Amps)

Model

Fuse Rating (Amps)

230V QBA1

2

120V QBA1

2

QBA2

2

QBA2

3.15

QBD1

2

QBD1

2

QBD2

2

QBD2

3.15

QBD4

3.15

QBD4

5

QBH2

2

QBH2

3.15

Routine safety tests If routine tests are to be made, we recommend a test of the integrity of the protective earth conductor and an insulation test at 500 V d.c. Routine flash tests are not recommended for any electrical equipment, because repeated high voltage tests degrade insulation materials.

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6.Guarantee and Service Guarantee When used in laboratory conditions and according to these working instructions, this product is guaranteed for THREE YEARS against faulty materials or workmanship. Extended warranty for years four and five can be purchased by contacting our sales department at [email protected].

Service There are no user serviceable parts inside the unit. For service return for repair to our Service Department in the UK or in other countries to our distributor. Please do not return the blocks. Service Address: Service Department Grant Instruments (Cambridge) Ltd Shepreth Cambridgeshire SG8 6GB England. Tel: +44 (0) 1763 260 811 Fax: +44 (0) 1763 262 410 E-mail: [email protected] At Grant we are continuously trying to improve the performance we offer our customers. If you have any feedback on Grant’s products or services we would like to hear from you. Please send all feed back to: Quality Manager Grant Instruments (Cambridge) Ltd Shepreth Cambridgeshire SG8 6GB England. Tel: +44 (0) 1763 260 811 Fax: +44 (0) 1763 262 410 E-mail: [email protected]

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7.Accessories

Only use genuine Grant products with your block heater. The following accessories are available from Grant Instruments, or our local distributor. Single Blocks

Double size blocks for QBA2,QBD2 and QBH

Grant Part no. Description

Grant Part no.

Description

QB-0 QB-10 QB-12 QB-13 QB-16 QB-18 QB-24 QB-50 QB-H QB-E0 QB-E1 QB-E2

QDP-H QDP-FL

0.2ml 96-well plate

Plain 10mm holes 12mm holes 13mm holes 16mm holes 18mm holes 24mm holes 50mm holes 0.2ml micro tube 0.5ml micro tube 1.5ml micro tube 2.0ml micro tube

EN

Polycarbonate safety covers QBL1 QBL2 QBL4

Cover for QBA1,QBD1 Cover for QBA2,QBD2,QBH2 Cover for QBD4

External Probe QBEP

External Pt1000 sensor

Special blocks can be made to order. Please contact Grant Instruments at [email protected] for details.

QBD, QBA, QBH, Operating Manual

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8.Specification Supply Specifications Voltage

Frequency

Power

QBA1 QBA2 QBD1 QBD2 QBD4 QBH2

230V ±10%

50-60Hz

200VA 350VA 200VA 350VA 700VA 350VA

QBA1L QBA2L QBD1L QBD2L QBD4L QBH2L

120V ±10%

50-60Hz

150VA 300VA 150VA 300VA 550VA 300VA

Stability @ 37 ºC within block

Uniformity @ 37 ºC within block

Number of blocks

Setting resolution ºC

Display resolution ºC

Adjustable overtemperature cut out

Heat up time 25 to 100 ºC minutes

External probe socket

Width x height mm

Max Temperature ºC

Minimum Setting Temperature ºC

Model variations QBA/QBAL

0

100

±1.0

±1.0

1&2

2

2

no

25

no

200 x100

QBD/QBDL

15

130

±0.1

±0.1

1,2&4

0.1

0.1

no

20

yes

200 x100

QBH/QBHL

15

200

±0.1

±0.1

2

0.1

0.1

yes

20

yes

200 x100

Block variations

Length

All block heaters are fitted with a thermal fuse which operates at a temperature of 230°C.

1 block

230

Heater power (watts) 230/110V 150/100

2 block

280

300/200

4 block

380

600/400

Operating Temperature Maximum relative humidity

5 to 40°C 80 % r.h. in room temperatures up to 31°C decreasing linearly to 50 % r.h. at 40°C

Altitude

Up to 6,500 feet (2,000 m) above sea level

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9.Compliance

WEEE Directive In Europe, at the end of its life the GR150, GP200 must be disposed of in accordance with the WEEE directive, For information regarding WEEE collections in the UK please contact our B2B Compliance Scheme directly on 01691 676 124 Grant Instruments complies fully with the Waste Electrical & Electronic Equipment (WEEE) regulations 2006. We are a member of the B2B compliance scheme (Scheme Approval Number WEE/MP3338PT/SCH), which handle our WEEE obligations on our behalf. Grant Instruments have been issued with a unique registration number by the Environmental Agency, this reference number is WEE/ GA0048TZ. For other countries please contact your equipment supplier. For General WEEE information please visit: www.b2bcompliance.org.uk

RoHS Directive All the products covered by this manual comply with the requirements of the RoHS Directive (Directive 2002/95/EC). This means the products are free of Lead and other hazardous substances covered by the directive.

Electrical safety and Electromagnetic compatibility All the products covered by this manual comply the the requirements of the Low Voltage Directive (2006/95/EC) for Electrical safety and the EMC directive (2004/108/EC) for Electromagnetic compatibility. See the Declaration of Conformity on the inside back page

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EN

Manufacturer

Equipment Name Equipment Description Directives Including Accessories CE mark first applied Applied Harmonised Standards

Grant Instruments (Cambridge) Ltd Shepreth Cambridgeshire SG8 6GB England Tel: +44 (0) 1763 260811 Fax: +44 (0) 1763 262410 Email: [email protected] www.grantinstruments.com

Printed in England -QBA - QBD –QBH –28089 /Version12 /DMN C43 / October 2012